Structural and Functional Investigations of the N-Terminal Ubiquitin Binding Region of Usp25.
Ubiquitin-specific protease 25 (Usp25) is a deubiquitinase that is involved in multiple biological processes. The N-terminal ubiquitin-binding region (UBR) of Usp25 contains one ubiquitin-associated domain, one small ubiquitin-like modifier (SUMO)-interacting motif and two ubiquitin-interacting motifs. Previous studies suggest that the covalent sumoylation in the UBR of Usp25 impairs its enzymatic ... activity. Here, we raise the hypothesis that non-covalent binding of SUMO, a prerequisite for efficient sumoylation, will impair Usp25's catalytic activity as well. To test our hypothesis and elucidate the underlying molecular mechanism, we investigated the structure and function of the Usp25 N-terminal UBR. The solution structure of Usp251-146 is obtained, and the key residues responsible for recognition of ubiquitin and SUMO2 are identified. Our data suggest inhibition of Usp25's catalytic activity upon the non-covalent binding of SUMO2 to the Usp25 SUMO-interacting motif. We also find that SUMO2 can competitively block the interaction between the Usp25Â UBR and its ubiquitin substrates. Based on our findings, we have proposed a working model to depict the regulatory role of the Usp25Â UBR in the functional display of the enzyme.
Mesh Terms:
Animals, Calorimetry, Chromatography, Gel, Dynamic Light Scattering, Escherichia coli, Humans, Mice, Models, Molecular, Mutation, Nuclear Magnetic Resonance, Biomolecular, Protein Binding, Protein Domains, Small Ubiquitin-Related Modifier Proteins, Solutions, Ubiquitin, Ubiquitin Thiolesterase
Animals, Calorimetry, Chromatography, Gel, Dynamic Light Scattering, Escherichia coli, Humans, Mice, Models, Molecular, Mutation, Nuclear Magnetic Resonance, Biomolecular, Protein Binding, Protein Domains, Small Ubiquitin-Related Modifier Proteins, Solutions, Ubiquitin, Ubiquitin Thiolesterase
Biophys. J.
Date: May. 23, 2017
PubMed ID: 28538147
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